Method of Preparation of PETN From Diluted HNO3
The method that you are going to learn in this manual is verfied, and by using this method you can efficiently prepare PETN from HNO3.
This report includes 3 different forumulas and and ratios for creating the chemical. Acid ratios are precisely calculated on data from PETN nitration graph and is forming to maximum 30% of water portion in nitration mixture. When H2SO4 is contained in nitration mixture, minimum ammount of water must be kept, or oxidation with small yields will occur.
So, the nitration mixture has 20% of water on nitration start and 30% at the end. Excess of HNO3 is used to controll ammount of reaction water. Only ammount of nitration mixture can be extended for lower mixture thickness. T
his book will guide you through the process of Preparing PETN From Diluted HNO3.
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